Organic Chemistry II
Laboratory Schedule, Spring 2009

Date	Experiment	Reading Assignment
Jan. 26-30	Lab Assignment and Check-In	None
Feb. 2-6	Mass Spectrometry I Determination of Molecular Formula	Read Sec. 15.3, p. 752, in your textbook. Mass Spec. I PowerPoint
Feb 9-13	Mass Spectrometry II Fragmentation Patterns	Re-read Sec. 15.3, p. 752, in your textbook. Mass Spec. II PowerPoint / Lecture Supplement
Feb. 16-20	Mass Spec. III Gas Chromatography-Mass Spec.	Identifying an Unknown Compound by GC-MS, Infrared Spectroscopy, IR Five Zones and GC-MS Lecture Supplement
Feb. 23-27	Dehydration of Cyclohexanol	REAC 712: Dehydration of Cyclohexanol
March 2-6	Nuclear Magnetic Resonance Spectroscopy I	1H NMR Spectroscopy I PowerPoint.   Read in text: Sec. 15.5-15.7, p.768-781.
March 9-13	Nuclear Magnetic Resonance Spectroscopy II	1H NMR Spectroscopy II PowerPoint. Read in text Sec. 15.7-15.8, p.781-794, and Sec. 15.11, p. 799. Peruse: Using 1H NMR Spectroscopy for Structure Determination (will be provided in lab)
March 16-20	Spring Break	HAVE FUN
March 23-27	Nuclear Magnetic Resonance Spectroscopy III	Read in text Sec. 15.10 and 15.11, p.796-802. 13C NMR Spectroscopy I PowewrPoint / Lecture Supplement (will be provided in lab) / Combined Spectroscopy Problems
Mar. 30-Apr. 3	Nuclear Magnetic Resonance Spectroscopy IV	During this lab period there will be a test on structure determination using NMR, IR spectroscopy and mass spectrometry.
April 6-10	No Lab
April 13-17	Oxidation of Methoxybenzyl Alcohol	SYNT 725: Oxidation of Alcohols. We will be performing the Semi-Microscale procedure.
April 20-24	Fischer Esterification	SYNT 713: Esterification; Review TECH 702: Microscale Techniques. Read Sec. 18.6, p. 986 in your textbook: Fischer Esterification.
April 27-May 1	Lab Check-Out	Study Organic Chemistry
May 4-8	No Lab	Study Organic Chemistry